arthur h. thomas company

1
NEW... fÂOtoaù. Model 38 Magne-Flash Evaporator Eliminates rotating seals with their difficulties • Magnetic spray action provides greater efficiency than rotating flask type 4946-M12. EVAPORATOR, Thomas Magne-Flash, Model 38.* Patented magnetic stir-spray principle of this instrument effects an evaporation rate significantly higher than that obtained with con- ventional rotating flask devices. New unitized design makes unit easier to use and safeguards operator against danger of vacuum-produced implosion of glassware with undetected flaws. Vigorous magnetic stirring action disperses solution in the 1000 ml evap- orating flask, which is heated by a water bath. Need for rotating seal is eliminated, permitting use of simple glass system with Τ joints. The greatly accelerated evaporation rate re- sults from the large surface of solution, which is dispersed as a constant spray of small droplets, continuously wetting flask wall. The required high speed stirring is made possible by patented double-magnet bar, driven by a powerful mag- netic stirrer. Lock-in effect of double magnet keeps bar in synchronization with magnetic drive at high speeds. Condenser flask collects up to 500 ml of solvent. •U.S. Patents No. 3,245,665; No. 3,306,829 Construction. Vacuum system is entirely of borosil- icate glass, connected by Τ joints. Solution to be con- centrated is placed in the evaporator flask or in the addition funnel, which has a Teflon stopcock for controlled addition. Evaporator water bath is heated by an immersion heater pad, sheathed in silicone rubber. Bath temperature is adjusted by a time- proportioning input controller. The water-jacketed vapor transfer tube conducts solvent vapors to the condenser flask in the cooling bath. Thermometers are provided for evaporator and condenser baths. The glassware is mounted on elevator-type support rack by which it can be raised or lowered, as a unit, into the heating and cooling baths in the base housing. In the raised position, the evaporator and condenser flasks can be easily installed and removed without affecting support or alignment of the vapor transfer tube. In the lowered position the greater part of each flask is surrounded by the stainless steel bath walls and the substantial aluminum base cabinet. The glass superstructure units are behind a meth- acrylate shield. Overall dimensions, 13 X 23 Χ 24Η inches high. 4946-M12. Evaporator, Thomas Magne-Flash, as de- scribed. For 115 volts, 50 or 60 cycles, a.c; 400 watts 350.00 7ΑΟΜΟΑ Bulletin 4946-M12 sent upon request. ARTHUR H. THOMAS COMPANY Scientific Apparatus and Reagents VINE STREET A T 3 R D · P. O. BOX 7 7 9 · PHILADELPHIA S, PA., U . S . A . Circle No. 87 on Readers' Service Card Π4Α · ANALYTICAL CHEMISTRY

Upload: doannhi

Post on 11-Feb-2017

213 views

Category:

Documents


0 download

TRANSCRIPT

NEW... fÂOtoaù. Model 38 Magne-Flash Evaporator

• Eliminates rotating seals

with their difficulties

• Magnetic spray action

provides greater efficiency

than rotating flask type

4946-M12.

EVAPORATOR, Thomas Magne-Flash, Model 38.* Patented magnetic stir-spray principle of this instrument effects an evaporation rate significantly higher than that obtained with con­ventional rotating flask devices.

New unitized design makes unit easier to use and safeguards operator against danger of vacuum-produced implosion of glassware with undetected flaws. Vigorous magnetic stirring action disperses solution in the 1000 ml evap­orating flask, which is heated by a water bath. Need for rotating seal is eliminated, permitting use of simple glass system with Τ joints.

The greatly accelerated evaporation rate re­sults from the large surface of solution, which is dispersed as a constant spray of small droplets, continuously wetting flask wall. The required high speed stirring is made possible by patented double-magnet bar , driven by a powerful mag­netic stirrer. Lock-in effect of double magnet keeps bar in synchronization with magnetic drive at high speeds. Condenser flask collects up to 500 ml of solvent. •U.S. Patents No. 3,245,665; No. 3,306,829

Construction. Vacuum system is entirely of borosil-icate glass, connected by Τ joints. Solution to be con­centrated is placed in the evaporator flask or in the addition funnel, which has a Teflon stopcock for controlled addition. Evaporator water bath is heated by an immersion heater pad, sheathed in silicone rubber. Bath temperature is adjusted by a time-proportioning input controller. The water-jacketed vapor transfer tube conducts solvent vapors to the condenser flask in the cooling bath. Thermometers are provided for evaporator and condenser baths.

The glassware is mounted on elevator-type support rack by which it can be raised or lowered, as a unit, into the heating and cooling baths in the base housing. In the raised position, the evaporator and condenser flasks can be easily installed and removed without affecting support or alignment of the vapor transfer tube. In the lowered position the greater part of each flask is surrounded by the stainless steel bath walls and the substantial aluminum base cabinet. The glass superstructure units are behind a meth-acrylate shield.

Overall dimensions, 13 X 23 Χ 24Η inches high. 4946-M12. Evaporator, Thomas Magne-Flash, as de­scribed. For 115 volts, 50 or 60 cycles, a.c; 400 watts 350.00

7ΑΟΜΟΑ

Bulletin 4946-M12 sent upon request.

ARTHUR H. THOMAS COMPANY Scientific Apparatus and Reagents

V I N E S T R E E T A T 3 R D · P. O . B O X 7 7 9 · P H I L A D E L P H I A S , P A . , U . S . A .

Circle No. 87 on Readers' Service Card Π 4 Α · ANALYTICAL CHEMISTRY